0.5 uL injection Injection Date Sample Name Acq. Operator Method Last changed 0x0000- 500000- 0- : C:\HPCHEM\1\METHODS\COMPNUC1.M 2/4/09 4:24:17 PM by (modified after loading) David Toft Alternate method for competing nucleophiles

laboratory (132B) FID1 A, (WACHTERALIKD) Cantane courts - 4000000- 3:500000 3000000 2500000 2000000 1500000- Sorted By Multiplier Dilution Sample Amount 0 : 2/4/09 4:38:37 M 1-Butylhalides : David Toft 1 2 3 : : Signal 1: FID1 A, Peak RetTime Type Width # [min] [min] : : ----|-‒‒‒‒‒‒‒‒‒‒‒‒‒‒‒--|--- 1.981 VV 2.527 VB 3.005 VB 1.5 Area Percent Report Height Area counts s [counts] Vial : Inj Volume: Manually -|--------| 0.0431 4.81925e6 3.72736e6 42.06241 0.0289 1.30990e6 9.02042e5 11.43281 0.0295 5.32823e6 3.54363e6 46.50478 1.14574e7 8.17303e6 Totals : Results obtained with enhanced integrator! *** End of Report *** cument 1 2/4/09 4:42:39 PM David Toft Signal 1.0000 1.0000 1.00000 [ng/ul] (not used in calc.) Duty Area 8 0 Br min Page 1 of 1