H₂CO
OH
OEt
CH3 CH₂
1. SOCI ₂. pyr
2. CH₂OH
+
3. CH₂CH₂CH₂MgBr (2 eq)
4. H₂0*
1. CH3CH₂CH₂CH₂NH₂, DCC
2. LAH
3. H₂O*
1. LDA, -30°C
2. CHyCH,CH,CH,C
+ Eto
OE!
OH¹
EIO ¹
Eto¹
Fig: 1