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Q1: MSE 110 Laboratory Manual Structure Characterization Properties Processing Performance Department of Materials Science and Engineering University of Arizona Tucson, AZ 85721 LAB 1: Atomic Spectra and Balmer's Experiment 1- Introduction: According to De Broglie's principle, particles with small masses and high velocity can exhibit quantum behavior. In effect, they behave like waves. Electrons orbiting around a nucleus indeed have wavelike characteristics. In particular, they interfere constructively to produce standing waves so that only the orbits which satisfy nλ= 2är are stable (where λ is the wavelength of the electron and r is the radius of the orbit). It derives that electrons can only exist on specific orbits with specific energies, as depicted for the simplistic Bohr hydrogen atom model in Fig. 1. E3 E2 hv Ef E1 hv-E-Ef Fig. 1: Left: Standing wave on a circular orbit. Right: Bohr hydrogen atom model. When an atom absorbs energy (for example in the form of an electric discharge), electrons can be promoted onto higher levels, but they eventually relax back down by re-emitting that energy in the form of a photon (Fig. 1). The photon energy if therefore a measure of the difference in energy between the atomic levels: hv Ef -Ei. The sum of all the photons emitted by an atom is called the "atomic spectrum” and contains information on all the electronic energy levels present in a given atom. = Balmer was the first to observe these atomic spectra back in 1885, although at the time he did not understand its relevance to quantization. Nevertheless, he was able to derive what is now known as the Rydberg constant which permits to quantify the difference in energy between electronic levels of the hydrogen atom. In this lab, you will use a modern spectrometer to duplicate Balmer's experiment and experimentally determine the value of the Rydberg constant. You will first assess the calibration and estimate the resolution of the spectrometer using a helium discharge lamp as a calibration standard. You will then use the spectrometer to measure the energy level of the hydrogen atom and derive an experimental value of the Rydberg constant. 2- Experimental Procedure: List of materials • An helium discharge lamp • A hydrogen discharge lamp A spectrometer Procedure Step 1: Calibration and resolution of the spectrometer 1- Log into the computer (click MSE110LAB) and open the SpectraSuite program. The software should display a flat spectrum (Fig. 2). 2- Bring the helium discharge lamp within an inch of the fiber connected to the spectrometer. 3- Turn on the lamp. A spectrum with multiple peaks should appear on the graph of the software. 4- Lower the Integration time (point A in Fig. 2) until the highest peak intensity is below the maxim of 4000 counts on the graph. Increase the Scans to Average (point B on Fig. 2) until the spectrum intensity stabilizes. 5- Save the spectrum (point C on Fig. 2). In the dialog box use the drop down menu to select the File Type as “Tab Delimited, No Header" (point D in Fig. 2). Browse to save the file on the Desktop. 6- Open Excel, browse for the file using "All Files" and open it. 7- Graph the spectrum on Excel. 8- From your data determine the wavelength resolution of the spectrometer. 9- Determine and record the wavelength of each peak at their maximum intensity. Step 2: Experimental derivation of the Rydberg constant. 1- Bring the hydrogen discharge lamp within an inch of the fiber connected to the spectrometer. 2- Turn on the lamp and lower the integration time as detailed in step 1. 3- Save and plot the spectrum with Excel as detailed in step 1. 4- Determine and record the position of the three peaks at their maximum intensity. A File View SpectrometProcessing Tools Window Help B Integration Time: Scans to 100 milliseconds 100 Boxcar A 1 Nonlinearity Data Sources RED Average: Width: Correction: Stray Light Correction: External Trigger: Normal II Strobe Lamp Enable: Electric Dark Correction: IK C Graph (A) x USB650 Q Q Q @ + 90 SATRI Acquisition Int time: 100ms, avg: 1, b No Pre-processor, Sco Result Properties Data Views Graph (A) Graph (A) Intensity (counts) 4000- 3000- 2000- SpectraSuite Save Spectrum ...Spectrometers Processing 0 USB2G40989 No Pre-processor, Scope Mode Filename: Browse... Spectrum View 120 100- 80- Desired Spectrum: Processed Spectrum File Type: OOI Binary Format Grams SPC CAMP-OX Tab Delimited 300 1000 Wavelength (nm) Tab Delimited, No Header D Save Close File name is required. 1000- Source: USB2G40989 400 500 Wavelength (nm): 1000.00 Oot Binary Format 600 700 Wavelength (nm) 800 900 1000 Fig. 2: View of the SpectraSuite software for collection of atomic spectra. ΜΕ 3- Calculations Knowing the wavelength resolution of the spectrometer, calculate the energy resolution (difference in energy between two adjacent measurement points), at 400 nm and 800nm. hc E = λ Express the energy resolution AE in Joules and in eV. Compare the values of the spectral line collected in step 1 to the National Institute of Standard and Technology values reported in Table 1. Intensity (relative) Wavelength (nm) 300 388.86 200 447.15 30 471.32 20 492.19 100 501.56 500 587.56 200 667.81 100 706.52 50 728.13 Table 1: Main lines of the atomic spectrum of helium from NIST. Estimate the Rydberg constant using the Balmer's relation: 1 λ = R H 1 22 - 1 n 2 Use Excel to plot versus λ (12/17) with n=3,4,5 and obtain the slope of the plot to derive the n Rydberg constant. Your report should include: 1- An Excel graph of atomic spectra for helium and hydrogen. 2- The energy resolution of the spectrometer at 400nm and 800nm in Joules and ev 3- A table comparing the values of helium spectral line collected experimentally to the standard values. 4- A discussion of whether the error on your measurement is within the wavelength resolution of the spectrometer. 5- A list of the spectral line for the hydrogen atom. 6- An Excel graph of versus 1 λ 1 1 and the derived Rydberg constant. 22 2 n 7- A discussion of how accurate your derivation is compared to the actual value and what could be the source of error./nHCP FCC lattice BCC measured 12.3mm a do 20mm 140m Measured do 45mm -70mm -> 17.3mm Calculated C21 mm-3 culculate ao 17.96mm CN 12 78.5% PPF B 44.66mm nighest density direction? Across me of the cube densest direction? atons Le (N 8712 CN PF PF atoms/u.c $74 PFF AFF Packmg Factor. 74.1% FCC BCC none/nSee Answer
Q2:5-9. Calculate the molarity and normality of the following: a. 80 μg/L HNO3 b. 135 µg/L CaCO3 c. 10 µg/L Cr(OH)₂ d. 1000 µg/L Ca(OH)₂See Answer
Q3:5-4. What is the concentration of chlorine (in mg/L) of household bleach that contains 5.25 percent by weight of Cl₂? Assume the density of water = 1,000 kg/m³.See Answer
Q4: ght atomic with as e aver S: 113 In, d 115 In, e aver- alculate otopes. nu of a al con- e atom. Bonding Forces and Energies whic 05 zamotan 100 2.15 Calculate the force of attraction between a Ca²+ and an O2- ion whose centers are separated by a y many ding distance of 1.25 nm. un Sen taken tance? ements atomic , what ecify? ers for in the ite the rons in ond to lowing Sonod sun ly ionic struc- ses? (H)22s22p63s23p64s¹ (c)2s22p 3s²3p63d¹04s²4p64d³5s² (02s²2p635² Th my off 2.14 (a) What electron subshell is being filled for the rare earth series of elements on the periodic table? (b) What electron subshell is being filled for the actinide series? 45-4p⁰ 2.16 The atomic radii of Mg and Fions are 0.072 and 0.133 nm, respectively. bood (a) Calculate the force of attraction between these two ions at their equilibrium interionic sepa- ration (i.e., when the ions just touch one another). plin (b) What is the force of repulsion at this same separation distance? BURSA 2.17 The orce of attraction between a divalent cation and a divalent anion is 1.67 X 10-8 N. If the ionic radius of the cation is 0.080 nm, what is the anion Gradius? 2.18 The net potential energy between two adjacent ions, EN, may be represented by the sum of Equations 2.9 and 2.11; that is, Thank you so much! EN (2.17) Calculate the bonding energy E, in terms of the pa- rameters A, B, and n using the following procedure: No, it's not. A B + " 0 5:59 ollowing ntly ionic on struc- ases? EN = and any Eo between the two ions. Calculate the bonding energy E, in terms of the pa- rameters A, B, and n using the following procedure: EN of the bonding energy (c) Mathematically determine the ro and Eo val- ues using the solutions to Problem 2.18, and com- pare these with the graphical results from part (b). 2.26 = → A B + r p" 2.20 Consider a hypothetical X-Yion pair for which e the equilibrium interionic spacing and bonding en- ergy values are 0.38 nm and -5.37 eV, respectively. If it is known that n in Equation 2.17 has a value of 8, using the results of Problem 2.18, determine explicit expressions for attractive and repulsive energies EA and ER of Equations 2.9 and 2.11. C 2.21 The net potential energy En between two adjacent ions is sometimes represented by the expression r 5G (2.17) + D exp(-) (2.18) Spr in which r is the interionic separation and C, D, 2.1 and p are constants whose values depend on the specific material. (a) Derive an expression for the bonding energy Eo in terms of the equilibrium interionic separa- tion Yo and the constants D and p using the follow- ing procedure: Mixe 2.25 + (i) Differentiate En with respect to r, and set the resulting expression equal to zero. Bon 2.27 +See Answer
Q5:You are expected to write a lab report on the experiment assigned to you by the module leader. The experiment could be one of the following that you have performed in Weeks 2 to 5 of the lab. 1) Residence time distribution for Tanks in Series 2) Degree of conversion and the reaction rate constant in a CSTR 3) Rate of settling in a vertical column 4) Level control in a liquid tankSee Answer
Q6: 2) Advances in molecular machinery have afforded various approaches toward performing macroscopic like tasks at the molecular level. Fort o mimick the motion of vehicles at the molecular level nano vehicles have been designed and developed. Nano worms are a design of a nano vehicles that mmick caterpillar-like motion. a) Is this approach toward molecular machines a bottom-upor top-down approach? Why? b) Why dould these molecules exhibit caterpillar-like motion? c) Would there be a directional motion of these molecules on a surface? If yes indicate the-expected direction of motion via arrows. d) Why does the motion of these molecules need to be studied on a surface?See Answer
Q7: 1) Nanochemistry focuses on designing and producing innovative materials and technologies.However there are concerns regarding safety and eco-impact a) Identify 2 areas where nano materials could have a strong impact in the future and describe how nano materials can be used in 2 types of applications within each of these areas. b) Explain 1 possible chemical approach that could be useful for reducing the cytotoxicity effects of toxic nanoparticles (i.e. CdSe QDs)? c) What would you think is most important in what concerns safety of nano materiaks forbio-nano applications: size, shape or surface? Explain your reasoning for your choice.See Answer
Q8: 1) Compute the molecular weight of the following compounds using the periodic table. C6H12O6 NaOH H₂S FeCl3 C6H5CH3See Answer
Q9: 4) Calculate the pH and pOH of a 0.001 M solution of sodium hydroxide (NaOH) at25 C. See Answer
Q10: Calculate the grams of oxygen formed through photosynthesis reaction of 1 mole of carbon dioxide. The photosynthesis reaction can be written as follows: \mathrm{H}_{2} \mathrm{O}+\mathrm{CO}_{2} \rightarrow \mathrm{C}_{6} \mathrm{H}_{12} \mathrm{O}_{6}+\mathrm{O}_{2}See Answer
Q11: Which of the three disubstituted benzene ringspolar? Use your data to justify your is more answer.See Answer
Q12: Fill in the table at the bottom of page three with the bond lengths from Task 1 (Comparing Single and Double Bonds in Cyclic Hydrocarbons) You can use either of the following methods: Print out the table, fill in the information,and upload an image of the completed table. • Write out the complete table by hand and upload an image of the completed table. Fill out the spreadsheet included in this table and upload the final table.See Answer
Q13: a) Draw the skeletal structure for both geometric isomers of 2-bromo-3-chloropent-2-ene.(in your answer, you must clearly label each of your structures as either E or Z)(3 b) A second compound, indene, was hydrated by reacting it with steam in the presence of an acid catalyst. Write the full mechanism for this reaction, showing all arrows and charges in your answer. Observe the reaction scheme shown below: c) For the products A, B and C: ) Draw the structure of the product ii) Deduce the IUPAC name of the product iii) State the name of the reaction that formed this productSee Answer
Q14: This question is about the theoretical compound tetrachloro(oxo)krypton, KrOCl4. ) Draw a dot and cross diagram for tetrachloro(oxo)krypton. b) Use your answer from Q1a) to deduce the molecular geometry of tetrachloro(oxo)krypton, c) The pressure of steam at 298K is 3.5kPa. 1.25g of water is put into a closed container that has a total volume of 1.50dm3. i) Deduce the number of moles of water that were vaporized. ii) Determine if there was any liquid water left in the container after vaporization.See Answer
Q15: Hair-dyes are cosmetic products that are used to either permanently or temporarily colour the hair.Ammonia is often used in hair dyes as it helps during the dyeing process. A cosmetic company is undergoing quality control checks to assess the percentage of ammonia in their2 new hair dyes. Dye A was expected to have (4.5+0.1)% ammonia and dye B was expected to have (7.5t0.1)%ammonia. 25.0g of dye A was transferred to a volumetric flask and made up to 250.0ml. with distilled water.The same was repeated for dye B. A 25.0mL portion of dye A was then transferred to separate conical flasks and titrated against a 0.125 M solution of sulphuric acid. The same was repeated for dye B. The results of experiment are show below: a) Use the information above to determine the percentage of ammonia in both dye A and B and state whether or not they meet the requirements. b) A student conducted an experiment to determine the volume of 1.50OM hydrochloric acid that was required to react completely with 1.75g of magnesium carbonate. The student deduced that exactly 13.88ml. were required. Show, by calculation, why this was incorrect and suggest the error this student made in the calculation.(4 marks)See Answer
Q16: Draw and name five different isomers of 1-chloro pentane? (20)See Answer
Q17: . Given these 3 compounds 2-methyl butanal, 2-chloro-1-cyclopentanone and 2,2 difluoro-propanoic acid. Draw each of these compounds. Use complete or condensed structure format only. (4 each)а. b. Name and draw the alcohols, that when oxidized, will form these compounds. (6 each)See Answer
Q18: Name this molecule. (4) Draw and name the two molecules used to synthesize this molecule (10) See Answer
Q19: 75. If 4.00g of nitrogen tetroxide and 4.00g of hydrazine (N2H) are mixed together to form dinitrogen tetroxide and hydrogen gas, determine the following a.limiting and excess reactants b. mass of product dinitrogen tetroxide. d. mass of excess reactant left overSee Answer
Q20: 69. Write the electron configuration and the boiling point constant is 0.512 °C/m.See Answer

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